华西口腔医学杂志

• 基础研究 • 上一篇    下一篇

深冷处理技术对口腔中熔铸造合金耐腐蚀性的影响

朱智敏,赵鹃,黄旭   

  1. 610041 四川大学华西口腔医学院
  • 收稿日期:2002-10-25 修回日期:2002-10-25 出版日期:2002-10-20 发布日期:2002-10-20

Effects of Cryotreat on the Corrosion Resistance of the Medium Melting-point Castable Alloy

Zhu Zhimin, Zhao Juan, Huang Xu   

  1. West China College ofStomatology, Sichuan University
  • Received:2002-10-25 Revised:2002-10-25 Online:2002-10-20 Published:2002-10-20

摘要:

目的:了解深冷处理技术用于处理口腔修复材料的效果及可行性。方法:将12个SDA-Ò型中熔铸造合金试件分为3组,分别为对照组、深冷处理组以及深冷处理加保温处理组,利用动电位极化曲线法,研究了SDA-Ò型中熔铸造合金经深冷处理后耐腐蚀性的变化。结果:¹深冷处理可以降低SDA-Ò型中熔合金的腐蚀电流,但对于耐点蚀性能没有影响。º从耐腐蚀性的角度而言,深冷处理后的保温处理对于SDA-Ò型中熔合金没有明显作用。结论:深冷处理技术是改善SDA-Ò型中熔合金耐腐蚀性的有效手段,初步证实该技术在口腔临床应用的可行性。

关键词: 深冷处理, 中熔铸造合金, 耐腐蚀性

Abstract:

Objective:The purpose of this studywas to investigate effects of cryotreaton the corrosion resistance of SDA-II mediummelt- ing-point castable alloy.Methods:12 samples were divided into three groups, including the control group, the cryotreated group and the cryotreated&post-cryogenic treated group. The cryotreating process was firstly dropping the temperature from room tem- perature to-170ewith dropping rate 3e/min, maintaining-170efor 2hrs, and then returning to ambient temperature with an increasing rate of 1e/min. The post-cryogenic process was maintaining the samples in 300efor 1hr. Finally, all sampleswere subjected to the electrochemical potentiodynamic polarization after immersed in the artificial saliva (ISO/TR10271:1993(E), pH 6.8) for 24hrs at ambient temperature. The exposing area of each sample was 10 mm@10 mm. The electrochemical tests were carried out in the artificial saliva under 37e, with the scanning rate of 20 mV/min, starting potential -200 mV below OCP and stopping current 10-3A. The corrosion currents (Icorr), the pitting corrosion potentials (Eb) and the potentiodynamic polarization curves were observed using the 283 electrochemical corrosion measuring system automatically.Results:For SDA-II medium melt- ing-point castable alloy, cryotreat reduced corrosion rate of the alloy, buthad no effecton the pitting corrosion potential. As far as the post-cryogenic treatment, it didnct affect the corrosion resistance.Conclusion:The results suggested that cryotreatwas an ef- fective procedure in enhancing the corrosion resistance of SDA-II mediummelting-point castable alloy, and itmay be applicable in prosthetic dentistry.

Key words: cryotreat, medium melting-point castable alloy, corrosion resistance