An investigation of the microstructure and mechanical properties of dental zirconia manufactured by digital light processing 3D printing

doi:10.7518/hxkq.2021.05.013

Abstract

Abstract: Objective

This study was performed to investigate the microstructure and mechanical properties of dental zirconia manufactured by digital light processing (DLP) 3D printing and the clinical application prospects of this material.

Methods

The experiment (DLP) group was zirconia manufactured by DLP 3D printing, and the control (MILL) group was milled zirconia. The density, grain size, and phase composition were measured to study the microstructure. Flexural strength was measured by using three-point bending tests, while Vickers hardness was determined through a Vickers hardness tester. Fracture toughness was tested using the single-edge V-notched beam method.

Results

Zirconia density of the DLP group was (6.019 8±0.021 3) g·cm^-3, and the average grain size was (0.603 0±0.032 6) μm, but without statistical difference with the corresponding values of the MILL group (P>0.05). Tetragonal phase was found in the X-ray diffraction patterns of the DLP and MILL groups. The flexural strength of the DLP group was (1 012.7±125.5) MPa, and Vickers hardness was (1 238.5±10.8) HV₁, which was slightly lower than that of the MILL group (P<0.05). The fracture toughness of the DLP group was (7.22±0.81) MPa·m^1/2, which was not statistically different from that of the MILL group (P>0.05).

Conclusion

Zirconia manufactured by DLP 3D printing had microstructure and mechanical properties similar to those of the milled zirconia. Only the flexural strength and the Vickers hardness of the experimental zirconia were slightly lower than those of the milled zirconia. Therefore, DLP-manufactured zirconia has a promising future for clinical use.

Key words: digital light processing, zirconia, microstructure, flexural strength, Vickers hardness, fracture toughness

CLC Number:

R 783.2

Mei Ziyu, Lu Yuqing, Lou Yuxin, Zhang Junjing, Sun Manlin, Yu Haiyang.. An investigation of the microstructure and mechanical properties of dental zirconia manufactured by digital light processing 3D printing[J]. West China Journal of Stomatology, 2021, 39(5): 576-581.

Figures/Tables 10

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References 11

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组别	密度/（g·cm^-3）	相对密度/%	晶粒尺寸/μm	晶相构成
DLP	6.019 8±0.021 3	99.009 9	0.603 0±0.032 6	四方相
MILL	6.038 2±0.011 5	99.312 5	0.591 1±0.033 0	四方相

组别	n	挠曲强度/MPa	Weibull模量	特征强度/MPa	R²
DLP	30	1 012.7±125.5	9.4	1 067.0	0.96
MILL	30	1 157.6±114.4	12.1	1 207.0	0.94

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