West China Journal of Stomatology
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WANG Si-qian, WANG Wei, DU Ruo-xi, ZHANG Da-feng, LIU Chuan-tong, MA Jianfeng
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Objective The objective of this study is to investigate the influence of mechanical properties and sintering performance by adding 5% weight percentage aids to nano-compound zirconia toughened alumina(ZTA) ceramics. Methods Micrometer Al2O3 and nanometer ZrO2(quality ratio 4 ∶ 1) were used to get 55% volume percentage slurry. Magnesium oxide and titanium oxide were taken as aids which were 5% weight percentage of the Al2O3 and ZrO2 powder. Five groups(number 0, 1, 2, 3, 4 group) were divided according to different proportion of aids. After gel-casting, the porcelain pieces were sintered at 1 150, 1 200, 1 300, 1 400, 1 450, 1 500, 1 600 ℃ for 2 hours. Static three-point flexure strength, line shrinkage, relative density were measured and scanning electron microscopy(SEM) was used to observe section. Results Number 1(MgO 1%, TiO2 4%) group had the highest bending strength. It was (401.78±19.50)MPa after sintering at 1 600 ℃ for 2 hours and was higher than 0 group (380.64±44.50)MPa. Bending strength became lower than 0 group when MgO was more than 2% or more than that weight percentage of ZTA powder. When MgO content was higher than 2% or more than that weight percentage, there was no difference in relative density raising rate between each sintering assistants groups. When the sintering temperature was higher than 1 200 ℃, all groups showed obvious line-shrinkage and the groups which contained sintering assistants were all was higher than 0 group. Conclusion Adding MgO and TiO2 aids from 1% to 4% weight percentage of ZTA will promote fritting and increase ZTA nano -compound ceramics mechanical properties. Adding 2% MgO aids or more than that weight percent will has no obvious help to increase the relative density raising rate of ZTA nano -compound ceramics and will degrade the mechanical properties of ZTA nano-compound ceramics.
Key words: zirconia toughened alumina ceramics, gel-casting, nano-compound ceramics
WANG Si-qian, WANG Wei, DU Ruo-xi, ZHANG Da-feng, LIU Chuan-tong, MA Jianfeng. Influence of MgO and TiO2 on mechanical properties of zirconia toughened alumina ceramics formed by gel-casting technique[J]. West China Journal of Stomatology.
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