West China Journal of Stomatology

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Influence of cryogenic treatment and age-hardening heat treatment on the microhardness of palladium-silver dental alloys

Zhao Yao1, Tong Xu1, Liu Jiajun2, Hao Zhichao2, Meng Yukun2.   

  1. 1. Chongqing Key Laboratory for Oral Diseases and Biomedical Sciences, Dept. of Prosthodontics, The Affiliated Hospital of Stomatology, Chongqing Medical University, Chongqing 401147, China; 2. State Key Laboratory of Oral Diseases, Dept. of Prosthodontics, West China Hospital of Stomatology, Sichuan University, Chengdu 610041, China
  • Online:2013-06-01 Published:2013-06-01

Abstract:

Objective   The purpose of this study was to investigate the influence of cryogenic treatment and age-hardening heat treatment on the micro-Vicker’s hardness of palladium-silver dental alloys. Methods     A low-gold content dental casting alloy composed of Ag-Pd-Cu-Au was prepared for this study. Experimental specimens according to standard requirements were prepared following a standard dental laboratory casting procedure, cast specimens were heated to 900 ℃ and quenched in ice water. The specimens were then divided into 4 groups. They were subsequently subjected to different treatments, including age-hardening heat treatment, cryogenic treatment, heat treatment combined with cryogenic treatment. The non-treated group was used as control. The micro-Vicker’s hardness value was examined. The significance of correlation was analyzed. Results   The micro-Vicker’s hardness of specimens after age-hardening heat treatment, cryogenic treatment, heat treatment combined with cryogenic treatment increased by 129%, 13% and 141%, respectively, compared with that of the non-treated control group. Conclusion   Age-hardening heat treatment and cryogenic treatment were effective in elevating the hardness of Ag-Pd-Cu-Au alloy.

Key words: dental casting alloy, age-hardening, cryogenic treatment, microhardness