关键词: 乙二胺四乙酸, 次氯酸钠, 自粘接树脂水门汀, 剪切强度

Abstract:

Objective  This study aims to evaluate the bond strength of a self-adhesive resin cement to dentin by ethylenediamine tetraacetic acid (EDTA) and NaClO. Methods  Twenty-seven freshly extracted non-carious human premolars were prepared to expose the buccal dentin and randomly divided into three groups: control group (A group), EDTA group (B group) and NaClO group (C group). All teeth were bonded to dentin using a self-adhesive resin cement after the teeth in the A group were processed with distilled water. The B and C group were processed with 3%EDTA and 1%NaClO, respectively. After 24 hours at 37 ℃ water, the shear bond strengths of the twenty-four specimens were measured. All statistical analysis was performed using SPSS 17.0 software package. Each fractured specimen was examined under dental microscope. Three new specimens were cut, and the morphologies of the cement-dentin interface were observed under scanning electron microscope (SEM). Results  The shear bond strength in the A group, B group and C group was (8.55±0.63), (8.47±0.56) and (12.97±0.59) MPa, respectively. The difference between A group and B group was no statistically significant (P>0.05), whereas the difference between C group and B group (or A group) was statistically significant (P<0.05). SEM observation of the cementdentin interface in the C group showed good adaptation, but resin tags were not observed. The other two groups showed poor bonding interface. Most of the fractured adhesive dentin surfaces exhibited cohesive failure in the A group and B group. All the fractured adhesive dentin surfaces exhibited cohesive failure in the C group. Conclusion  1% NaClO can increase the bond strength of self-adhesive resin cement to dentin, but 3%EDTA has no effect.

Key words: ethylenediamine tetraacetic acid, NaClO, self-adhesive resin cement, shear bond strength